HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → HCID 12509451, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | HCID 53421801 | HCID 53421801 | — |
| Product | HCID 12509451 | HCID 12509451 | 76.9% |
Reaction Steps
1,4-Dichloro-3-buten-2-one (0.0556 kg, 0.4 mole) and diethyl malonate (0.064 kg, 0.4 mole) were condensed under identical conditions to those described in Example 1(b) to give the title compound 0.0865 kg (77%; purity, g.l.c., 87.85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362880 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-b30f4203052a4456ba4fa70c3e9da280 |
| Source note | uspto-grants-1982_12 |