HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzophenone → {4-Methoxy-2-[(prop-2-en-1-yl)oxy]phenyl}(phenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzophenone | HCID 3102 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | {4-Methoxy-2-[(prop-2-en-1-yl)oxy]phenyl}(phenyl)methanone | HCID 14227056 | — |
Reaction Steps
The ether was prepared as in the preceding example from 100 grams (0.45 moles) benzophenone, 61 grams (0.45 moles) K2CO3, 2.5 grams (0.45 moles) allyl bromide and 200 ml of acetone. The product (pale yellow oil) was isolated after 8 hours reflux and was rearranged without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362895 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-657ab2441ae34359a4589aa239874bca |
| Source note | uspto-grants-1982_12 |