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HRID1902379

反应详情

EQUATION

反应方程式

HRID 1902379 的结构方程式

REACTANTS

反应物

4
结构：O=C(c1ccccc1)c1ccccc1
HCID3102

Benzophenone

C13H10O

结构：CCOCC
HCID3283

Diethyl Ether

C4H10O

结构：C=CCBr
HCID7841

Allyl bromide

C3H5Br

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

PRODUCTS

生成物

1
结构：C=CCOc1cc(OC)ccc1C(=O)c1ccccc1
HCID14227056

{4-Methoxy-2-[(prop-2-en-1-yl)oxy]phenyl}(phenyl)methanone

C17H16O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

The ether was prepared as in the preceding example from 100 grams (0.45 moles) benzophenone, 61 grams (0.45 moles) K2CO3, 2.5 grams (0.45 moles) allyl bromide and 200 ml of acetone. The product (pale yellow oil) was isolated after 8 hours reflux and was rearranged without further purification.

WORKUP

后处理

  1. customThe product (pale yellow oil) was isolated after 8 hours
  2. temperaturereflux
  3. customwas rearranged without further purification