HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 20515434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 20515452 | HCID 20515452 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20515434 | HCID 20515434 | — |
Reaction Steps
2.73 g (0.01 mole) of ethyl 3-(2-aminophenyl)amino-1,5-dimethyl-1H-pyrrole-2-carboxylate in a solution of 0.25 g (0.011 mole) of sodium in 40 ml of dry ethanol are boiled under reflux for 2 hours. After the mixture has cooled, it is neutralized carefully with acetic acid; the solvent is stripped off in vacuo, and the yellowish residue is recrystallized from dioxane. Yield: 1.9 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04363816 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-7d9bc16a46834b4ba8f3575b028c767c |
| Source note | uspto-grants-1982_12 |