HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-3-Methylthio-1,5,10,10a-tetrahydrothiazolo[3,4-b]isoquinolinium iodide → HCID 22822257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-3-Methylthio-1,5,10,10a-tetrahydrothiazolo[3,4-b]isoquinolinium iodide | HCID 12874874 | — |
| Reactant | Thieno[2,3-c]pyridin-3-amine | HCID 15342498 | — |
| Product | HCID 22822257 | HCID 22822257 | 68.2% |
Reaction Steps
By following the procedure of Example 2, but using (S)-3-methylthio-1,5,10,10a-tetrahydrothiazolo[3,4-b]isoquinolinium iodide (10.1 g) and 3-aminothieno[2,3-c]pyridine (6.4 g) as the starting materials, (S)-3-[(thieno[2,3-c]pyrid-3-yl)imino]-1,5,10,10a-tetrahydrothiazolo[3,4-b]isoquinoline (6.4 g) is obtained in the form of white crystals, m.p.=180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04363909 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-11ed046b25b642b3ac6997b62f5442f2 |
| Source note | uspto-grants-1982_12 |