HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-3-Methylthio-1,5,10,10a-tetrahydrothiazolo[3,4-b]isoquinolinium iodide → HCID 22822248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-3-Methylthio-1,5,10,10a-tetrahydrothiazolo[3,4-b]isoquinolinium iodide | HCID 12874874 | — |
| Reactant | Isoquinolin-8-amine | HCID 13927912 | — |
| Product | HCID 22822248 | HCID 22822248 | 71.1% |
Reaction Steps
By following the procedure of Example 2, but using (S)-3-methylthio-1,5,10,10a-tetrahydrothiazolo[3,4-b]isoquinolinium iodide (18.2 g) and 8-aminoisoquinoline (10.9 g) as the starting materials, (S)-3-(isoquinol-8-ylimino)-1,5,10,10a-tetrahydrothiazolo[3,4-b]isoquinoline (11.8 g) is obtained in the form of pale yellow crystals, m.p.=206° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04363909 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-1f98494f16e94f9cb265c4983a0560ad |
| Source note | uspto-grants-1982_12 |