Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2,4,5-Trichloronitrobenzene | HCID 6983 | — |
| Reactant | Potassium phenoxide | HCID 23670670 | — |
| Product | HCID 20514529 | HCID 20514529 | — |
Reaction Steps
A mixture of 1 mol of 2,4,5-trichloro-1-nitrobenzene, 2 mols of potassium phenolate and phenol was heated for 1 hour at 165° C., and the reaction product was isolated as described in Example A(a), yielding the title compound, m.p. 95° C. (recrystallized from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04364875 |
|---|
| Source dataset | uspto-grants-1982_12 |
|---|
| ORD ID | ord-2897972a2d1442288e8cca2d4b894d27 |
|---|
| Source note | uspto-grants-1982_12 |
|---|