Ethylenediamine → HCID 12881157, compound

Participants

Reaction Conditions

Reaction Steps

6.83 gm of 6-chloro-4-nitro-1,3-diphenoxy-benzene were dissolved in 15 ml of dioxane, an excess of 1,2-diamino-ethane was added to the solution, and the mixture was heated for 12 hours at 70° C. Thereafter, the reaction mixture was worked up as in Example 3, and the reaction product was purified by recrystallization from ethanol. 6.1 gm (88% of theory) of the white crystalline compound of the formula ##STR10## having a melting point of 255° C. (decomp.) were obtained.

Provenance & Evidence