HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 13001827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl acetoacetate | HCID 7757 | — |
| Reactant | HCID 13001826 | HCID 13001826 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13001827 | HCID 13001827 | — |
Reaction Steps
16.4 g of 2-(3-methoxyphenyl)-propionaldehyde, 23.2 g of methyl acetoacetate and 2.1 ml of NH3 (33% strength) in 50 cm3 of ethanol were heated under reflux for 4 hours. After the mixture had cooled, the product crystallised out. It was purified by recrystallisation from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04364952 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-480efe456c0c4393bbdf1dc3ed32466d |
| Source note | uspto-grants-1982_12 |