HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitroethane → HCID 54050540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 4-Butylbenzaldehyde | HCID 70988 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54050540 | HCID 54050540 | — |
Reaction Steps
A stirred solution of 4-butylbenzaldehyde (13.5 g), nitroethane (9.0 ml) and butylamine (1.6 ml) in ethanol (20 ml) was heated under reflux for 6 hours and evaporated. The residue was distilled under vacuum to give 1-(4-butylphenyl)-2-nitropropene (bp 124°-125° C./0.15 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04364956 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-9d78cbf07f6042fd9b5a90e5018b7d7e |
| Source note | uspto-grants-1982_12 |