HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 12940617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Iodine chloride | HCID 24640 | — |
| Reactant | HCID 2683980 | HCID 2683980 | — |
| Reactant | Potassium Iodate | HCID 23665710 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12940617 | HCID 12940617 | — |
Reaction Steps
In connection with the foregoing Reaction Scheme, p-phenoxyphenyl benzoate of formula VI is either reacted with iodine monochloride in aqueous acetic acid or treated with potassium iodide and an oxidizing agent, for example potassium iodate or hydrogen peroxide, in aqueous methanol, to afford the iodo derivative of formula VII. This iodo derivative is saponified by heating in alkali, for example alcoholic sodium hydroxide, to give p-(p-iodophenoxy)phenol of formula V.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04365991 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-71b785b8752d4d14bc90a0768b13d650 |
| Source note | uspto-grants-1982_12 |