Phenol → p-Isopropenylphenol
Reaction equation
C1(O)C=CC=CC=1.[CH:8]([C:11]1[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=1)([CH3:10])[CH3:9]>O>[C:8]([C:11]1[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=1)([CH3:10])=[CH2:9]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
In this example, the procedure employed in Example 1 was repeated by passage of the mixture of air, phenol, water, and para-isopropylphenol over the pretreated catalyst, this time at a temperature of about 400°-480° C. for 37 hours. A total of 23 cuts were taken yielding a total volume of about 330 ml product whose conversions to the para-isopropenylphenol were between about 25-30%.
Sources & evidence
- ORD record
- ord-5d4aa21d6ce54bf1ae0d571f04673461
- Source dataset
- uspto-grants-1982_12
- Patent number
- US04366089
Reaction notes
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