Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Bromohexadecane | HCID 8213 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Methyl-1,3-benzoxazol-6-ol | HCID 676504 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12886752 | HCID 12886752 | 100.5% |
Reaction Steps
18.0 g of 6-hydroxy-2-methylbenzoxazole synthesized from Synthesis 1, 36.6 g of 1-bromohexadecane, 24.0 g of potassium carbonate and 120 ml of N,N-dimethylformamide were mixed with stirring at 90° C. for 4.5 horus. Solids were removed from the reacting solution, and the filtrate was poured into 500 ml of methanol. The separated crystals were separated by filtration to obtain 45.0 g of 6-hexadecyloxy-2-methylbenzoxazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04366226 |
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| Source dataset | uspto-grants-1982_12 |
|---|
| ORD ID | ord-2a3af5d4e92e441db66278a20e5bac2f |
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| Source note | uspto-grants-1982_12 |
|---|
