HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 4-Pentyl-3-fluoroanisole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 1,1-Ethanediol | HCID 151211 | — |
| Reactant | 4-Valeryl-3-fluoroanisole | HCID 20514273 | — |
| Product | 4-Pentyl-3-fluoroanisole | HCID 20514278 | — |
Reaction Steps
4-Valeryl-3-fluoroanisole (14.1 g), hydrazine hydrate (8.6 ml) potassium hydroxide (4.4 g) and 1:1 dihydroxyethane (84 ml) were reacted together as described in Example 1. 4-Pentyl-3-fluoroanisole was isolated as a colourless oil b.pt 77° C. at 0.1 mm. The product showed 1 spot only on tlc using dichloromethanepetrol (1:1) as solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04366330 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-b14077b30c89452d8b052ebadd29d10c |
| Source note | uspto-grants-1982_12 |