Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Hexamethylenetetramine | HCID 4101 | — |
| Reactant | HCID 20467693 | HCID 20467693 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20467692 | HCID 20467692 | 79.6% |
Reaction Steps
A mixture of 2-chloro-3,5-bisfluorosulphonylthiophene (8.5 g), hexamine (8.5 g) and methanol (90 ml) was stirred under reflux for one hour. The mixture was cooled to 25° C., poured into dilute sulphuric acid and extracted with ethyl acetate to give the product as an oil (6.3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04435320 |
|---|
| Source dataset | uspto-grants-1984_03 |
|---|
| ORD ID | ord-36934874ada444b2936876130b56ed7d |
|---|
| Source note | uspto-grants-1984_03 |
|---|
