HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylphosphonic Acid → HCID 178443263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylphosphonic Acid | HCID 15295 | — |
| Reactant | HCID 178443264 | HCID 178443264 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 178443263 | HCID 178443263 | 120.5% |
Reaction Steps
n-Dodecyl thiouronium chloride (8.0 g), phenylphosphonic acid (10 g), and 200 ml of 50/50 (v/v) ethanol/water mixture were heated overnight and then cooled. After filtering and recrystallizing from water-methanol-ethanol, approximately 11.1 g of n-dodecyl thiouronium phenyl phosphonate was isolated (m.p. 154°-156° C.). Chemical analysis and infrared spectra confirmed n-dodecyl thiouronium phenylphosphonate formation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04435381 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-0fd66c78152b4a328078aca6958f8bcd |
| Source note | uspto-grants-1984_03 |