HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13194908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 8-Hydroxy-3,4-dihydronaphthalen-1(2H)-one | HCID 584353 | — |
| Solvent | 2-Methoxyethanol | HCID 8019 | — |
| Product | HCID 13194908 | HCID 13194908 | — |
Reaction Steps
To the solution heated to 80° C. of 3.2 g of 8-hydroxy 1-tetralone and 20 ml of epichlorohydrin in 20 ml of 2-methoxy ethanol is added 1.8 g of sodium hydroxide and the mixture is heated to reflux for 1 hour. Water is added and the mixture is extracted with methylene chloride. The organic phase is separated, dried and the solvent is evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04435426 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-1f1dc561fc2d4992940ae3bc4f72fa44 |
| Source note | uspto-grants-1984_03 |