HRID1903274

反应详情

EQUATION

反应方程式

HRID 1903274 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 5.6 g. of 1-phenyl-3-azabicyclo[3.1.0]hexane hydrochloride, 12.9 g. of aluminum chloride and 6.2 g. of propionyl chloride in 55 ml. of dichloromethane is reacted as described in Example 57, to give 4.5 g. of the desired product, m.p. 191°-193° C.

WORKUP

后处理

  1. additionA mixture of 5.6 g
  2. customto give 4.5 g