HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionyl chloride → HCID 20468337, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionyl chloride | HCID 62324 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 1-Phenyl-3-azabicyclo[3.1.0]hexane hydrochloride | HCID 12719843 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20468337 | HCID 20468337 | — |
Reaction Steps
A mixture of 5.6 g. of 1-phenyl-3-azabicyclo[3.1.0]hexane hydrochloride, 12.9 g. of aluminum chloride and 6.2 g. of propionyl chloride in 55 ml. of dichloromethane is reacted as described in Example 57, to give 4.5 g. of the desired product, m.p. 191°-193° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04435419 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-0852d275431840e9915a1297d9177f5d |
| Source note | uspto-grants-1984_03 |