HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → Methoxyethyldiethanolamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | N-Allyl-2,2'-iminodiethanol | HCID 41439 | — |
| Reactant | Ethanol, 2-methoxy-, 1-(4-methylbenzenesulfonate) | HCID 86977 | — |
| Product | Methoxyethyldiethanolamine | HCID 13635719 | — |
Reaction Steps
The above named compound was prepared by the procedure described in Example 1 for N-allyldiethanolamine, using 0.5 mol of diethanolamine, 0.55 mol of 2-methoxyethyl tosylate and 29.15 g of sodium carbonate. After workup the crude product was fractionally distilled and the fraction boiling from 90°-110° at 0.1 mm was collected. N-(2-Methoxyethyl)diethanolamine, i.e.,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436664 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-08189a7f83094e9997ab30e056d35700 |
| Source note | uspto-grants-1984_03 |