HRID1903388

反应详情

EQUATION

反应方程式

HRID 1903388 的结构方程式

PROCEDURE

实验过程

The title compound was prepared as described above for N-allyldiethanolamine in Example 1 except that 2-methoxyethoxyethyl tosylate was used (0.55 mol, 150.9 g) in a 0.5 mol preparation. The pure diol whose formula is shown below was obtained (49.8 g, 48%) on fractional distillation at 129°-131° C. (0.04 mm):

WORKUP

后处理

  1. customin a 0.5 mol preparation
  2. custombelow was obtained (49.8 g, 48%)
  3. distillationon fractional distillation at 129°-131° C. (0.04 mm)