HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Allyl-2,2'-iminodiethanol → 2,2'-{[2-(2-Methoxyethoxy)ethyl]azanediyl}di(ethan-1-ol)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Allyl-2,2'-iminodiethanol | HCID 41439 | — |
| Reactant | HCID 11076628 | HCID 11076628 | — |
| Product | 2,2'-{[2-(2-Methoxyethoxy)ethyl]azanediyl}di(ethan-1-ol) | HCID 13635723 | — |
Reaction Steps
The title compound was prepared as described above for N-allyldiethanolamine in Example 1 except that 2-methoxyethoxyethyl tosylate was used (0.55 mol, 150.9 g) in a 0.5 mol preparation. The pure diol whose formula is shown below was obtained (49.8 g, 48%) on fractional distillation at 129°-131° C. (0.04 mm):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436664 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-00593ba9d30d4b0892dcb3dd130175ef |
| Source note | uspto-grants-1984_03 |