HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20268172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 20268177 | HCID 20268177 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 20268172 | HCID 20268172 | — |
Reaction Steps
A solution of 4 g of 1-(4-methoxycarbonylbutyl)-3-methyl-2-(1-imidazolyl)indole in 40 ml of n-butanol is saturated with ammonia and heated on a steam bath in a pressure bottle for 3 days. The reaction mixture is evaporated to dryness and the product is crystallized to yield the 1-[4-carbamoylbutyl]-3-methyl-2-(1-imidazolyl)indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436746 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-f6e074535f9645dd9623da6ebaed24d0 |
| Source note | uspto-grants-1984_03 |