HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20467555, compound → Idazoxan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20467555 | HCID 20467555 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | Idazoxan | HCID 54459 | — |
Reaction Steps
2-(1,4-benzodioxan-2-yl)imidazoline acetate (1.0 g) is dissolved in a solution of 1 ml 50% aqueous sulfuric acid in 10 ml ethanol, and the solution evaporated to dryness. The product is suspended in ethanol and filtered, air dried and recrystallized from methanol/acetone to yield 2-(1,4-benzodioxan-2-yl)imidazoline: HSO4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436914 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-6448b057c989457a8e1aecdf8b4c6611 |
| Source note | uspto-grants-1984_03 |