HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Phenyl-1-propenyl)aniline → 3-(3-Phenylpropyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Phenyl-1-propenyl)aniline | HCID 54042989 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(3-Phenylpropyl)aniline | HCID 427307 | 92% |
Reaction Steps
A solution of 3-(3-phenyl-1-propenyl)aniline (3.6 g) in 50 ml of ethanol was subjected to catalytic reduction using 1 g of 10% palladium-carbon. After removal of the catalyst by filtration, the solvent was removed under reduced pressure. The residue was distilled under reduced pressure to give 3.3 g of 3-(3-phenylpropyl)aniline (yield, 92%). B.P. 122°-126° C./0.08 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04437880 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-14973120f72e4eb5953e84b360c0baf4 |
| Source note | uspto-grants-1984_03 |