HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 23438954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 2-methyl-5-phenylthiophene | HCID 7578805 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 23438954 | HCID 23438954 | — |
Reaction Steps
To a boiling solution of 2-methyl-5-phenylthiophene (2g) in dry CCl4 (100 ml) was rapidly added N-bromosuccinimide (1.94 g) and dibenzoylperoxide (0.15 g). After heating under reflux for 30 min., the mixture was cooled and filtered. Evaporation in vacuo gave the title compound as an oil (1.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04438111 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-0902d85f48444f24ad68a2af63c4a5d5 |
| Source note | uspto-grants-1984_03 |