Hydrochloric Acid → HCID 70510479, compound

HRID 1903750Notes

Reaction equation

[C:1]([C:3]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16](=[O:22])[CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[C:4]=1[O:5][CH2:6][CH:7]([OH:10])[CH2:8][Cl:9])#[N:2].Cl>>[ClH:9].[C:1]([C:3]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16](=[O:22])[CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[C:4]=1[O:5][CH2:6][CH:7]([OH:10])[CH2:8][NH:15][CH:11]([CH3:12])[CH3:4])#[N:2]

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 20466863HCID 20466863, compound

Product 1

HCID 70510479HCID 70510479, compound

Procedure

From 12.9 gm (0.04 mol) of 1-(2-cyano-6-hexanoylamino-phenoxy)-3-chloro-2-propanol and 13.6 ml (0.16 mol) of isopropylamine, 5.3 gm of amino-alcohol were obtained, which were converted into the hydrochloride by the addition of HCl. Yield: 4.7 gm; M.p.: 107° C.

Sources & evidence

ORD record: ord-759151d3a7b74e32b154526d8c3610b8
Source dataset: uspto-grants-1984_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04438143

Reaction notes

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