HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 20402882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 573583 | HCID 573583 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 20402882 | HCID 20402882 | — |
Reaction Steps
The 1-azaspiro[5.5]undecane starting material can be prepared by the method described by H. Hodjat, et al., in J. Heterocyclic Chem., 9, 1081 (1972). This starting material is treated with benzoyl chloride in pyridine to form the N-benzoyl-1-azaspiro-[5.5]undecane, shown at the beginning of step 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04438130 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-389e3b295f164e5dafcf5cb9c57ebe6f |
| Source note | uspto-grants-1984_03 |