HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13290543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13290538 | HCID 13290538 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13290543 | HCID 13290543 | — |
Reaction Steps
A mixture of 3.7 g of 1, 0.39 g of sodium hydroxide and 50 ml of ethanol was refluxed for two hours, then it was cooled to room temperature, acidified with hydrochloric acid and extracted with ether. Concentration of the ether extract gave 2, as a white solid, m.p.: 181°-182° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04439226 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-95eb83fcdf71499eb43802964162dd18 |
| Source note | uspto-grants-1984_03 |