HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15589123, compound → HCID 20456650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15589123 | HCID 15589123 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20456650 | HCID 20456650 | — |
Reaction Steps
A solution of 17 g of 10B in 100 ml of tetrahydrofuran was treated with hydrogen (40 psi hydrogen pressure, Parr-shaker, 10% palladium-on-charcoal catalyst) to give methyl 2-(4-(2-amino-4-(trifluoromethyl)phenylamino)phenoxy)-3-methoxypropionate (10C), as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04439226 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-79274dbdd76249ea925fe3d9382effc9 |
| Source note | uspto-grants-1984_03 |