HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl orthoacetate → HCID 13290549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Reactant | HCID 20456650 | HCID 20456650 | — |
| Product | HCID 13290549 | HCID 13290549 | — |
Reaction Steps
A solution of 7 g of 10C in 25 ml of triethyl orthoacetate was refluxed for 4 hours. The resulting mixture was concentrated in a rotary evaporator and chromatographed over silica gel to give 10, as a viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04439226 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-c7b9bb2ee66341a6803dcf22b725194d |
| Source note | uspto-grants-1984_03 |