HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 13290548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13290552 | HCID 13290552 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13290548 | HCID 13290548 | — |
Reaction Steps
A solution of 2.4 g of 12 and 0.25 g of sodium hydroxide in 50 ml of aqueous ethanol was refluxed for one hour, and extracted with ether. The extract was dried and concentrated. The residue was crystallized from ether-hexane to give 13, as a white solid, m.p.: 67°-68° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04439226 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-9b46802ee94f42039665730613d504db |
| Source note | uspto-grants-1984_03 |