HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4,5,6-Tetrahydrophthalic anhydride → N-(3-Hydroxy-4-chlorophenyl)-3,4,5,6-tetrahydrophthalimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4,5,6-Tetrahydrophthalic anhydride | HCID 12475 | — |
| Reactant | 5-Amino-2-chlorophenol | HCID 80676 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | N-(3-Hydroxy-4-chlorophenyl)-3,4,5,6-tetrahydrophthalimide | HCID 12769235 | — |
Reaction Steps
Employed 47.5 g of 3-hydroxy-4-chloroaniline (0.33 mol); 38.2 of 3,4,5,6-tetrahydrophthalic anhydride (0.25 mol) and 350 ml of glacial acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04439229 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-409fc4fa12124257a8cc85edb33c9516 |
| Source note | uspto-grants-1984_03 |