HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 20465944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | HCID 13194789 | HCID 13194789 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20465944 | HCID 20465944 | 84% |
Reaction Steps
To a solution of 1 g of 3-benzenesulfonamido-N-[2-(5-dimethylaminomethylfuran-2-ylmethylthio)ethyl]benzamide in 15 ml of ethanol, a solution of 0.3 g of oxalic acid in 10 ml of ethanol is added. The salt which precipitates is filtered, dried and crystallized in 10 ml of 95% ethanol. Thus, 1 g of 3-benzenesulfonamido-N-[2-(5-dimethylaminomethylfuran-2-ylmethylthio)ethyl]benzamide oxalate is obtained as a vitreous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04439444 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-2c10054358a14621ab0398e9651e1fc9 |
| Source note | uspto-grants-1984_03 |