化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl 2-(4-nitrophenyl)butanoate → Ethyl 2-(4-aminophenyl)butanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 2-(4-nitrophenyl)butanoate | HCID 237528 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Ethyl 2-(4-aminophenyl)butanoate | HCID 12692883 | 94.3% |
反応手順
A solution of 9.13 g (0.0385 mole) of ethyl 2-(4-nitrophenyl)-n-butyrate in 150 ml of ethanol was subjected to hydrogenation in the presence of palladium black catalyst to give 7.51 g (0.0363 mole, 94% yield) of ethyl 2-(4-aminophenyl)-n-butyrate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04439448 |
| 出典データセット | uspto-grants-1984_03 |
| ORD ID | ord-285fcc7aa4b8467e976b87e80cd03ada |
| 出典メモ | uspto-grants-1984_03 |