HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 178430934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | HCID 178430933 | HCID 178430933 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178430934 | HCID 178430934 | 49.3% |
Reaction Steps
14.9 g of Compound [2-a] was benzenesulfonylated in the same manner as described in Step 1-h using 12 g of benzenesulfonyl chloride in 50 ml of pyridine and 20 ml of dimethylacetamide to obtain 10.8 g of Compound [2-b].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04439513 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-754f4af5e7284516a5e30adfdcced668 |
| Source note | uspto-grants-1984_03 |