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HRID1904026

反应详情

EQUATION

反应方程式

HRID 1904026 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1ccccc1
HCID7369

Benzenesulfonyl chloride

C6H5ClO2S

结构：Cc1c(N=Nc2ccc(CO)cc2)c(O)n(C)c(=O)c1C#N
HCID178430933

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(N=Nc2ccc(COS(=O)(=O)c3ccccc3)cc2)c(O)n(C)c(=O)c1C#N
HCID178430934

未命名化合物

收率 49.3%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

结构：CC(=O)N(C)C
溶剂HCID31374

Dimethylacetamide

C4H9NO

PROCEDURE

实验过程

14.9 g of Compound [2-a] was benzenesulfonylated in the same manner as described in Step 1-h using 12 g of benzenesulfonyl chloride in 50 ml of pyridine and 20 ml of dimethylacetamide to obtain 10.8 g of Compound [2-b].