Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-Hexadecanoylamino-4-methoxyethoxymethoxy-1-naphthol | HCID 131713445 | — |
| Reactant | HCID 178430934 | HCID 178430934 | — |
| Product | HCID 178443074 | HCID 178443074 | 70.6% |
Reaction Steps
5 g of Compound [1-f] was dissolved in 30 ml of dried diglime and to the solution was added 0.48 g of a 50% oily sodium hydride. Then, 4.4 g of Compound [2-b] was added and the mixture was stirred at 80° C. for 1.5 hours. By subjecting the same treatment as described in Step [1-i], 5.5 g of Compound [2-c] was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04439513 |
|---|
| Source dataset | uspto-grants-1984_03 |
|---|
| ORD ID | ord-9ac3f14169fa4a38b615efed18c6f3d2 |
|---|
| Source note | uspto-grants-1984_03 |
|---|
