Sodium Hydroxide → HCID 74088766, compound

Participants

Reaction Steps

28.2 g of ethyl 2-(2-tritylamino-4-thiazolyl)-2-(2-bromoethoxyimino)-acetate were added to a mixture of 6 g of sodium hydroxide pastilles in 280 ml of absolute ethanol and the mixture was stirred at room temperature for 65 hours and was vacuum filtered. The recovered product was washed with ethanol and dried under reduced pressure to obtain 29.2 g of the syn isomer of sodium 2-(2-tritylamino-4-thiazolyl)-2-(2-bromoethoxyimino)-acetate, solvated at 12%.

Provenance & Evidence