HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azepane → 1-(azepan-1-yl)octan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azepane | HCID 8119 | — |
| Reactant | Octanoyl chloride | HCID 8124 | — |
| Product | 1-(azepan-1-yl)octan-1-one | HCID 246824 | 68% |
Reaction Steps
In a manner similar to that described in Example 1, octanoyl chloride (16.26 g, 0.1M) was treated with hexahydro-1H-azepine (9.92 g, 0.1M). Work up and distillation of the residue gave 15.3 g (68%) of product, b.p. 122/0.8 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837026 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-58ba5aae3d1442228bd6a60aa643af18 |
| Source note | uspto-grants-1989_06 |