HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Ethoxy-1-ethylethoxy)-benzyl bromide → 2-t-butyl-4-chloro-5-[4-(2-ethoxy-1-ethylethoxy)-benzyloxy]-3(2H)-pyridazinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Ethoxy-1-ethylethoxy)-benzyl bromide | HCID 14671809 | — |
| Reactant | 2-tert-Butyl-4-chloro-5-hydroxypyridazin-3(2H)-one | HCID 54686946 | — |
| Product | 2-t-butyl-4-chloro-5-[4-(2-ethoxy-1-ethylethoxy)-benzyloxy]-3(2H)-pyridazinone | HCID 14671810 | 24.8% |
Reaction Steps
Procedures similar to those in Preparation Example 8 were carried out by using 2.0 g of 2-t-butyl-4-chloro-5-hydroxy-3(2H)-pyridazinone and 3.1 g of 4-(2-ethoxy-1-ethylethoxy)-benzyl bromide to obtain 1.0 g of the aimed compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837217 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-77bd14a7fc494bff9c29a9a57cdfd1b1 |
| Source note | uspto-grants-1989_06 |