HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Methyl-4-(trifluoromethyl)-5-thiazolecarbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methyl-4-(trifluoromethyl)-1,3-thiazole-5-carboxylic acid | HCID 1486080 | — |
| Product | 2-Methyl-4-(trifluoromethyl)-5-thiazolecarbonyl chloride | HCID 14601081 | — |
Reaction Steps
0.50 g of 2-methyl-4-trifluoromethylthiazole-5-carboxylic acid was added to 5 ml of thionyl chloride and reaction was carried out for 2 hours under reflux. After the reaction, the reaction mixture was concentrated to obtain 0.54 g of 2-methyl-4-trifluoromethylthiazole-5-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837242 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-304908544a1449b7aab3d6ad64b7afa6 |
| Source note | uspto-grants-1989_06 |