HCID 13590265, compound → HCID 14459388, compound

Participants

Reaction Steps

Utilising the procedure described in Example 1c and employing α-(4,4-dimethylpentyl)-1H-imidazole-1-ethanol in lieu of α-[[(4-methoxyphenyl)methoxy]methyl]-1H-imidazole-1-ethanol yielded a crude product which was purified by column chromatography (silica gel, chloroform) to yield 6,6-dimethyl-1-(1H-imidazol-1-yl)-2-heptanone as a colourless crystalline solid, having a melting point of 45°-46° C. (ether-hexane) and the following structural characteristics:

Provenance & Evidence