HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178526458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 6-Nitroindazole | HCID 24239 | — |
| Reactant | Sodium Hypochlorite | HCID 23665760 | — |
| Product | HCID 178526458 | HCID 178526458 | 95% |
Reaction Steps
To a mixture of 6-nitroindazole (1.63 g) and 6N sodium hydroxide (2.08 ml) was added 5.25% w/v sodium hypochlorite (17.86 ml). After stirring for 30 minutes, filtration, and washing with 1N sodium hydroxide, 1-sodio-3-chloro-6-nitroindazole (2.08 g, 95%) was obtained as a solid; mp >270° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837235 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-bf33b6b4b62e4751b48992ccad28cc7e |
| Source note | uspto-grants-1989_06 |