HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → HCID 20039277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | Tris(4-chlorophenyl)phosphine | HCID 70874 | — |
| Product | HCID 20039277 | HCID 20039277 | 91.7% |
Reaction Steps
A mixture of 2.08 g (5.69 mmol) of tris(4-chlorophenyl)phosphine and 1.03 g (5.53 mmol) of methyl tosylate was allowed to react for 1 hr at 125° C. A total of 2.80 g (5.07 mmol, 91.7%) of product was obtained, which was further purified by recrystallization from 97:3 toluene-ethanol. Analyses: mp 176.5°-177.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837392 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-371e6ee2b1fb401eae7d93af1b5fcefc |
| Source note | uspto-grants-1989_06 |