HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → HCID 20039305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | Tris(4-trifluoromethylphenyl)phosphine | HCID 139448 | — |
| Product | HCID 20039305 | HCID 20039305 | 73.4% |
Reaction Steps
A mixture of 5.25 g (11.3 mmol) of tris(4-trifluoromethylphenyl)phosphine and 2.43 g (13.0 mmol) of methyl tosylate were allowed to react for 2 hr at 135° C. A total of 5.41 g (8.29 mmol, 73.4%) of product was obtained, which was further purified by recrystallization from toluene-ethanol. Analyses: mp 185.0°-185.8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837392 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-de26e74edf8e4eef9516fe23e927b129 |
| Source note | uspto-grants-1989_06 |