HRID1904567

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID94784

Phosphorochloridic acid, dibutyl ester (8CI)(9CI)

C8H18ClO3P

HCID517096

Cyanic acid, sodium salt

CNNaO

PRODUCTS

生成物

HCID12583220

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Analogously to Example 1, 200 g of dibutoxyphosphinic acid chloride were reacted with 58 g of sodium cyanate in 350 ml of absolute acetonitrile. 142 g of a faintly yellowish liquid (69% of theory) having a boiling point of 80°-83° C./0.67 Pa were isolated.

WORKUP

后处理

customwere isolated