HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorochloridic acid, dibutyl ester → Dibutoxyphosphinic acid isocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorochloridic acid, dibutyl ester | HCID 94784 | — |
| Reactant | Sodium Cyanate | HCID 517096 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Dibutoxyphosphinic acid isocyanate | HCID 12583220 | — |
Reaction Steps
Analogously to Example 1, 200 g of dibutoxyphosphinic acid chloride were reacted with 58 g of sodium cyanate in 350 ml of absolute acetonitrile. 142 g of a faintly yellowish liquid (69% of theory) having a boiling point of 80°-83° C./0.67 Pa were isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04839254 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-7affca2c8d2c47d3adbfb36826a21016 |
| Source note | uspto-grants-1989_06 |