HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14068929, compound → HCID 14068939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14068929 | HCID 14068929 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14068939 | HCID 14068939 | — |
Reaction Steps
Following the procedure of Example 3, a solution of 3-isopropyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.0]hexane-2,4-dione in 100 ml of ethanol is hydrogenated in the presence of 0.17 g of 5% palladium on carbon and worked up, affording the title compound which melts at 160°-163° C. after recrystallisation from ethyl acetate/petroleum ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04839379 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-8a038a4a50814785bcd5a300cba3f4be |
| Source note | uspto-grants-1989_06 |