Hydrazine hydrate (1:1) → HCID 13576831, compound

Participants

Reaction Steps

To the N-benzenesulphonyl-9-acetamide (Example 10) (0.15 g) was added with stirring hydrazine hydrate (4 cm3) and the mixture heated to reflux under anhydrous conditions. After 24 hours all solid had dissolved to give a clear orange solution. All solvents were removed under high vacuum (<30° C.) to give after trituration with water (10 cm3) and acetone (2×10 cm3) an orange solid.

Provenance & Evidence